Header menu link for other important links
X
Thermal conductivity of precursor derived Si-B-C-N ceramic foams using Metroxylon sagu as sacrificial template
, Adhimoolam Bakthavachalam Kousaalya, B.T.N. Sridhar
Published in Elsevier Ltd
2015
Volume: 41
   
Issue: 1
Pages: 1163 - 1170
Abstract
Thermolysis of as-cast polyorganoborosilazane resulted in the formation of porous monolith of Si-B-C-N ceramic. However the addition of varying amounts of Metroxylon sagu (30-60 wt%) to polyorganoborosilazane, on thermolysis, resulted in Si-B-C-N foams. Thermo-gravimetric analysis of M. sagu revealed complete decomposition at 850 °C. Spark plasma sintering of Si-B-C-N was carried out at 1600 °C at a pressure of 30 MPa for 5 min in vacuum to obtain highly dense compacts. The obtained Si-B-C-N foam was found to be amorphous while the SPS-processed samples were observed to be highly crystalline. The geometrical density of the foam was found to vary from 0.4 to 0.25 g/cm3 with increase in sago content along with the presence of both closed and open cells. The thermal conductivity of the foam and SPS-processed samples showed varying trends with increasing temperature due to the amorphous and crystalline nature of the samplesrespectively. © 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
About the journal
JournalData powered by TypesetCeramics International
PublisherData powered by TypesetElsevier Ltd
ISSN02728842
Open AccessNo
Concepts (19)
  •  related image
    Amorphous silicon
  •  related image
    CERAMIC FOAMS
  •  related image
    Ceramic materials
  •  related image
    Crystalline materials
  •  related image
    Gravimetric analysis
  •  related image
    Silicon
  •  related image
    Sintering
  •  related image
    Spark plasma sintering
  •  related image
    Starch
  •  related image
    Thermogravimetric analysis
  •  related image
    As-cast
  •  related image
    Crystalline nature
  •  related image
    HIGHLY DENSE
  •  related image
    In-vacuum
  •  related image
    Increasing temperatures
  •  related image
    Open-cell
  •  related image
    POROUS MONOLITHS
  •  related image
    SACRIFICIAL TEMPLATES
  •  related image
    Thermal conductivity