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Large-area graphene-based thin films using rapid reduction of graphene-oxide
Published in
2013
Volume: 8692
   
Abstract
In the present study, we propose a method to fabricate large-area graphene-based thin films using rapid low-temperature reduction of graphene-oxide. Large area (∼17.5 sq.cm.) graphene oxide (GO) thin films are fabricated by vacuum filtration of GO solution synthesized by the modified Hummers' method. The graphene-oxide thin films are reduced in a MTS testing machine equipped with a controlled atmosphere furnace. Reduction is carried out at temperatures from 200°C to 400°C, for different time durations. The fabricated reduced GO thin films are characterized using powder x-ray diffraction and energy-dispersive x-ray spectroscopy. The reduced graphene oxide thin films show decreased interlayer spacing and higher carbon-to-oxygen ratio. Conductivity measurements show an increase in conductivity by over five orders of magnitude compared to GO. This method offers a scalable new way of fabricating conductive large-area graphene-based thin films. © 2013 SPIE.
About the journal
JournalProceedings of SPIE - The International Society for Optical Engineering
ISSN0277786X
Open AccessNo
Concepts (14)
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    Conductivity measurements
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    ENERGY DISPERSIVE X-RAY SPECTROSCOPY
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    INTERLAYER SPACINGS
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    LOW-TEMPERATURE REDUCTION
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    Orders of magnitude
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    Powder x ray diffraction
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    Reduced graphene oxides
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    THERMAL REDUCTION
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    Composite films
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    Energy dispersive spectroscopy
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    Graphene
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    Sensors
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    X ray diffraction
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    Thin films