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An efficient and mild synthetic strategy for the total synthesis of selaginpulvilin D has been reported. A highly chemoselective enyne–alkyne dehydro Diels–Alder reaction has been employed for the construction of the tricyclic fluorene framework present in the natural product selaginpulvilin D. An improved overall yield (10.5%) has been achieved for selaginpulvilin D, starting from commercially available m-anisaldehyde in 9 linear, operationally simple synthetic transformations.
Journal | Data powered by TypesetOrganic & Biomolecular Chemistry |
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Publisher | Data powered by TypesetRoyal Society of Chemistry (RSC) |
Open Access | No |