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Ultra-high pressure densification and properties of nanostructured SiC
Branko Matovic, Fatima Zivic, Slobodan Mitrovic, Dragan Prsic, Vesna Maksimovic, Tatjana Volkov-Husovic, , Nina Daneu
Published in Elsevier
2016
Volume: 164
   
Pages: 68 - 71
Abstract

Cubic SiC nano-powder particles were synthesized by a sol-gel process with an average grains size of 9.5 nm which were subsequently densified by using a high-pressure "anvil-type with hollows" apparatus at a pressure of 4 GPa in order to obtain nanostructured bulk ceramic compacts. The density obtained was >98% at a sintering temperature of 1500°C with a holding time of only 60 s. The calculation of the average crystallite size (D) was performed on the basis of the full width at half maximum intensity (FWHM) of the XRD peaks. Williamson-Hall plots were used to separate the effect of the size and strain in the nanostructured SiC compacts. Sintered nanostructured SiC ceramic exhibits hardness and elastic modulus of 32-420 GPa respectively. Wear properties were investigated and the average value of dynamic friction coefficient obtained was 0.16. © 2015 Elsevier B.V.

About the journal
JournalData powered by TypesetMaterials Letters
PublisherData powered by TypesetElsevier
ISSN0167577X
Open AccessNo
Concepts (15)
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    Ceramic materials
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    Crystallite size
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    Friction
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    Nanoparticles
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    Sintering
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    Sol-gel process
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    DYNAMIC FRICTION COEFFICIENT
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    FULL WIDTH AT HALF MAXIMUM INTENSITIES
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    HARDNESS AND ELASTIC MODULUS
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    SIC CERAMICS
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    Sintering temperatures
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    Structural
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    WILLIAMSON-HALL PLOT
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    X-RAY TECHNIQUES
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    Silicon carbide