Header menu link for other important links
X
Structural, functional and mechanical properties of spark plasma sintered gadolinia (Gd2O3)
Eranezhuth Wasan Awin, Soumya Sridar, Rajashekhar Shabadi,
Published in Elsevier Ltd
2016
Volume: 42
   
Issue: 1
Pages: 1384 - 1391
Abstract
Powder particles of gadolinia were spark plasma sintered at varied temperatures between 1400 °C and 1600 °C. High-density samples free of any sintering additives were obtained at the highest sintering temperature and the samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) including density measurements. The contact angle measurements and translucence studies implied the sintered samples to be hydrophobic and translucent respectively. The nanohardness values enhanced up to ∼88% with increase in sintering temperature from 1400 °C to 1600 °C. Young's modulii determined using nanoindentation varied from 126 GPa to 169 GPa for the samples sintered at the lowest and highest temperatures respectively. The theoretical Young's modulus was also determined using first principle calculations which were eventually used for fracture toughness calculations. The fracture toughness values of the sintered samples were calculated using the indentation crack length method (ICL) and compared with the crack opening displacement (COD) method. © 2015 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
About the journal
JournalData powered by TypesetCeramics International
PublisherData powered by TypesetElsevier Ltd
ISSN02728842
Open AccessNo
Concepts (16)
  •  related image
    Cracks
  •  related image
    Elastic moduli
  •  related image
    Indentation
  •  related image
    Scanning electron microscopy
  •  related image
    Sintering
  •  related image
    Spark plasma sintering
  •  related image
    X ray diffraction
  •  related image
    CRACK OPENING DISPLACEMENTS
  •  related image
    First principle calculations
  •  related image
    Fracture toughness values
  •  related image
    Gadolinia
  •  related image
    Highest temperature
  •  related image
    INDENTATION CRACK
  •  related image
    SINTERING ADDITIVES
  •  related image
    Sintering temperatures
  •  related image
    Fracture toughness