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Optical calibration for nanocalorimeter measurements
, Burke B.G., Holness A.E., Wilthan B., Hanssen L., Weihs T.P., LaVan D.A.
Published in Elsevier BV
2011
Volume: 522
   
Issue: 1-2
Pages: 60 - 65
Abstract

We describe a method for calibration of nanocalorimeters from 573 K to 873 K, using resistive heating and optical pyrometry for temperature measurement. A platinum strip suspended on a silicon nitride membrane serves as both heater and temperature sensor. The calibration described here, relating resistance to temperature, enables subsequent temperature measurement. Measurements of the emissivity of as-deposited and annealed platinum thin films were also performed as a function of wavelength and temperature; these measurements are needed to correct the temperature recorded using the pyrometer. The calibration was validated by measurement of the melting point of a pure aluminum film; the melting point established with a Gaussian fit to the dT/dt data agreed within 0.1% (0.7 K) at 933.5 K. The melting point established from the minimum in the dT/dt plot agreed within 0.6% (5.5 K) at 933.5 K. Finite element modeling was used to characterize the temperature distribution.

About the journal
JournalData powered by TypesetThermochimica Acta
PublisherData powered by TypesetElsevier BV
Open AccessNo