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Mo2NiB2-type {Gd, Tb, Dy)2Ni2.35Si0.65 and La2Ni3-type {Dy, Ho}2Ni2.5Si0.5 compounds: Crystal structure and magnetic properties
Published in Academic Press Inc.
2015
Volume: 225
   
Pages: 368 - 377
Abstract
The crystal structure of new Mo2NiB2-type {Gd, Tb, Dy}2Ni2.35Si0.65 (Immm, No. 71, oI10) and La2Ni3-type {Dy, Ho}2Ni2.5Si0.5 (Cmce No. 64, oC20) compounds has been established using powder X-ray diffraction studies. Magnetization measurements show that the Mo2NiB2-type Gd2Ni2.35Si0.65 undergoes a ferromagnetic transition at ∼66 K, whereas isostructural Tb2Ni2.35Si0.65 shows an antiferromagnetic transition at ∼52 K and a field-induced metamagnetic transition at low temperatures. Neutron diffraction study shows that, in zero applied field, Tb2Ni2.35Si0.65 exhibits c-axis antiferromagnetic order with propagation vector K=[1/2, 0, 1/2] below its magnetic ordering temperature and Tb magnetic moment reaches a value of 8.32(5) μB at 2 K. The La2Ni3-type Dy2Ni2.5Si0.5 exhibits ferromagnetic like transition at ∼42 K with coexisting antiferromagnetic interactions and field induced metamagnetic transition below ∼17 K. The magnetocaloric effect of Gd2Ni2.35Si0.65, Tb2Ni2.35Si0.65 and Dy2Ni2.5Si0.5 is calculated in terms of isothermal magnetic entropy change and it reaches a maximum value of -14.3 J/kg K, -5.3 J/kg K and -10.3 J/kg K for a field change of 50 kOe near 66 K, 52 K and 42 K, respectively. Low temperature magnetic ordering with enhanced anisotropic effects in Tb2Ni2.35Si0.65 and Dy2Ni2.35Si0.65 is accompanied by a positive magnetocaloric effect with isothermal magnetic entropy changes of +12.8 J/kg K and ∼+9.9 J/kg K, respectively at 7 K for a field change of 50 kOe. © 2015 Elsevier Inc.
About the journal
JournalJournal of Solid State Chemistry
PublisherAcademic Press Inc.
ISSN00224596
Open AccessNo
Concepts (29)
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    Antiferromagnetism
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    Crystal structure
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    Crystallography
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    Dysprosium compounds
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    Entropy
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    Ferromagnetic materials
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    Ferromagnetism
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    Isotherms
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    Magnetic field effects
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    Magnetic moments
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    Magnetic properties
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    Magnetic structure
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    Magnetism
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    Magnetocaloric effects
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    NEEL TEMPERATURE
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    Neutron diffraction
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    RARE EARTH COMPOUNDS
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    Silicon
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    Temperature
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    X ray diffraction
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    Antiferro-magnetic interactions
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    Antiferromagnetic orderings
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    Antiferromagnetic transition
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    Field induced metamagnetic transitions
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    Isothermal magnetic entropy change
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    Magnetic ordering temperatures
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    Magnetization measurements
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    NEUTRON DIFFRACTION STUDIES
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    Nickel