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Microstructural characterisation of friction stir processed aluminium
Published in
2011
Volume: 27
   
Issue: 7
Pages: 1163 - 1169
Abstract
Friction stir processing was carried out on commercially pure aluminium, and a detailed microstructural characterisation was performed by electron backscattered diffraction and transmission electron microscopy. Friction stir processing resulted in significant grain refinement with narrow grain size distribution. The microstructure showed fine and equiaxed grains, with some ultrafine grains being also observed. Electron backscattered diffraction studies showed majority of the boundaries to be high angle, confirming the occurrence of dynamic recrystallisation (DRX). Transmission electron microscopy observations revealed dislocation arrangement into subgrain boundaries, grains having different dislocation densities and in different stages/degrees of recovery. Electron backscattered diffraction analysis also revealed a progressive transformation of sub-grain boundaries into high angle grain boundaries. A multimechanism of dynamic recovery, continuous DRX and discontinuous DRX seems to be operating during the process. The microstructure is not affected by changing the rotation speed from 640 to 800 rev min -1, except that the grain size was marginally larger for higher rotational speed. © 2011 Institute of Materials, Minerals and Mining.
About the journal
JournalMaterials Science and Technology
ISSN02670836
Open AccessNo
Concepts (31)
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    DISLOCATION ARRANGEMENT
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    Dislocation densities
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    Dynamic recovery
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    DYNAMIC RECRYSTALLISATION
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    Electron backscattered diffraction
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    ELECTRON BACKSCATTERED DIFFRACTION ANALYSIS
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    Equiaxed grains
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    Friction stir
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    Friction stir processing
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    Grain size
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    Grain size distribution
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    High angle grain boundaries
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    MICROSTRUCTURAL CHARACTERISATION
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    PURE ALUMINIUM
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    Rotation speed
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    Rotational speed
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    SUBGRAIN BOUNDARIES
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    Transmission electron
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    TRANSMISSION ELECTRON MICROSCOPY OBSERVATION
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    Ultra fine grain
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    Aluminum
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    Electron diffraction
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    Electrons
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    Friction
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    Grain boundaries
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    Grain size and shape
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    Microstructure
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    Recrystallization (metallurgy)
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    Transmission electron microscopy
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    Tribology
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    Grain refinement