Header menu link for other important links
X
Influence of mode of electrodeposition, current density and saccharin on the microstructure and hardness of electrodeposited nanocrystalline nickel coatings
, , Suresh Krishnamoorthy Seshadri, Govindan Sundararajan
Published in Elsevier
2016
Volume: 291
   
Pages: 130 - 140
Abstract
The main purpose of the present work is to study the influence of current density, deposition mode and the presence of saccharin as an additive on the microstructure, sulfur content, grain size and microhardness of nanocrystalline Ni coatings. Towards this purpose, nanocrystalline nickel (Ni) coatings were deposited at various current densities in Watt's bath using direct, pulse and pulse reverse current (PRC) electrodeposition and subsequently characterized for sulfur content, grain size and hardness. It was observed that, the current density has no influence on the grain size/hardness of nanocrystalline Ni coatings in direct and pulsed current electrodeposition mode. However, the grain size increased from ~ 20 to ~ 200 nm with decrease in current density in PRC mode of deposition. In addition a substantial change in microstructure and texture of PRC Ni coatings was also evident. The experimental results have been rationalized based on the adsorption-desorption type of mechanism during electrodeposition. © 2016 Elsevier B.V..
About the journal
JournalData powered by TypesetSurface and Coatings Technology
PublisherData powered by TypesetElsevier
ISSN02578972
Open AccessNo
Concepts (23)
  •  related image
    Coatings
  •  related image
    Current density
  •  related image
    Deposition
  •  related image
    Electrodeposition
  •  related image
    Electrodes
  •  related image
    Grain size and shape
  •  related image
    Hardness
  •  related image
    Microstructure
  •  related image
    Nanocrystals
  •  related image
    Nickel
  •  related image
    Sugar substitutes
  •  related image
    Sugars
  •  related image
    Sulfur
  •  related image
    Textures
  •  related image
    ADSORPTION DESORPTION
  •  related image
    DEPOSITION MODES
  •  related image
    Grain size
  •  related image
    NANO-CRYSTALLINE NICKEL
  •  related image
    NANOCRYSTALLINE NI
  •  related image
    NANOCRYSTALLINE NICKEL COATINGS
  •  related image
    PULSED-CURRENT ELECTRODEPOSITION
  •  related image
    Reverse currents
  •  related image
    Nickel coatings