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Evidence for ferromagnetic clusters at room temperature in Dy and Mn site co-substituted compounds: Dy0.55Sr0.45Mn1-xFexO3
Published in Elsevier Ltd
2019
Volume: 792
   
Pages: 411 - 417
Abstract
Polycrystalline compounds of Dy0.55Sr0.45Mn1-xFexO3 (x = 0.0–1.0: 0.2) were prepared by high temperature solid state reaction route. All the compounds were found to have orthorhombic structure with Pnma space group with four formula units per unit cell. However, for high iron content corresponding to 0.8 and 1.0, some impurity phases were present. Raman modes of the substituted compounds were found to shift to higher wave numbers as compared to x = 0.0. All the compounds displayed insulating property with variable range hopping type of conduction. Mössbauer spectroscopy studies performed at room temperature revealed the presence of both trivalent and tetravalent iron ions for high concentrations of iron. Sextet pattern observed for high iron content suggested the presence of a magnetic phase even at room temperature. Temperature variation of magnetization showed paramagnetic behavior in the high temperature region (>100 K) and displayed variety of magnetic structures below 100 K. Effective magnetic moments (μeff.) of the compounds were determined by fitting the molar susceptibility data in the paramagnetic state to Curie-Weiss law. Experimental effective magnetic moment values were found to be larger than the calculated μeff. values revealing ferromagnetic cluster formation. © 2019 Elsevier B.V.
About the journal
JournalData powered by TypesetJournal of Alloys and Compounds
PublisherData powered by TypesetElsevier Ltd
ISSN09258388
Open AccessNo
Concepts (26)
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    Dysprosium
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    Dysprosium compounds
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    Ferromagnetic materials
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    Ferromagnetism
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    High temperature applications
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    Iron
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    Iron compounds
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    Magnetic moments
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    Magnetic structure
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    Magnetization
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    Manganites
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    Metal ions
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    Mossbauer spectroscopy
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    Paramagnetism
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    Solid state reactions
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    Strontium compounds
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    X ray diffraction
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    Effective magnetic moments
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    Ferromagnetic clusters
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    HIGH TEMPERATURE SOLID-STATE REACTION
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    Orthorhombic structures
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    POLYCRYSTALLINE COMPOUNDS
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    Ssbauer spectroscopies
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    Temperature variation
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    Variable range hopping
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    Manganese compounds