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Cyclophanes, XLIV synthesis of 4,5,12,13-tetraformyl[2.2]paracyclophane and its bis-acetal
Published in
2000
   
Issue: 15
Pages: 2699 - 2701
Abstract
4,5,12,13-Tetraformyl[2.2]paracyclophane (1f) has been prepared for the first time by the cycloaddition of 4,4-diethoxy-2-butynal (3) to 1,2,4,5-hexatetraene (2) under various conditions and hydrolysis of the initially produced bis-acetals 5a and 5b. An X-ray crystal structural analysis of 5a is reported.
About the journal
JournalEuropean Journal of Organic Chemistry
ISSN1434193X
Open AccessNo
Concepts (11)
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    Acetal derivative
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    Aldehyde derivative
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    PARACYCLOPHANE DERIVATIVE
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    Article
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    Chemical analysis
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    Chemical structure
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    Crystal
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    Crystal structure
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    Structure analysis
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    Synthesis
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    X ray crystallography